C₈₂H₈₁Cl₂N₁₃O₂₄P₂

Base Information

• Chemical Name: C₈₂H₈₁Cl₂N₁₃O₂₄P₂
• CAS No.: 74231-45-1
• Molecular Formula: C₈₂H₈₁Cl₂N₁₃O₂₄P₂
• Molecular Weight: 1765.47
• Mol file: 74231-45-1.mol

Synonyms:C₈₂H₈₁Cl₂N₁₃O₂₄P₂

Chemical Property of C₈₂H₈₁Cl₂N₁₃O₂₄P₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₈₂H₈₁Cl₂N₁₃O₂₄P₂

There total 1 articles about C₈₂H₈₁Cl₂N₁₃O₂₄P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dmtbzCtp(qcl)bzCtp(qcl)BzAt (74219-87-7) → C82H81Cl2N13O24P2 (74231-45-1)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; at 0 ℃; for 0.25h;

DOI:10.1021/jo01304a042

Reference yield: 80.0%

C82H81Cl2N13O24P2 (74231-45-1) + O-8-(5-chloroquinolyl) phosphate (71933-71-6) → qclpbzCtp(qcp)bzCtp(qcl)bzAt (74219-89-9)

Guidance literature:

With (PySe)2; triphenylphosphine; In pyridine; for 15h; Ambient temperature;

DOI:10.1021/jo01304a042

Reference yield:

C82H81Cl2N13O24P2 (74231-45-1) → cytidylyl-(3'->5')-cytidylyl-(3'->5')-adenosine (2866-39-9)

Guidance literature:

With hydrogenchloride; ammonia; zinc(II) chloride; Yield given. Multistep reaction; 1) pyridine, water, 24h room temperature 2) 5h 50 deg C 3) 18h 20 deg C;

DOI:10.1021/jo01304a042

upstream raw materials:

dmtbzCtp(qcl)bzCtp(qcl)BzAt

Downstream raw materials:

qclpbzCtp(qcp)bzCtp(qcl)bzAt

cytidylyl-(3'->5')-cytidylyl-(3'->5')-adenosine