Technology Process of C23H17NO5
There total 6 articles about C23H17NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: n-butyllithium; carbon dioxide / tetrahydrofuran / 1 h / -78 °C
1.3: 2 h / -78 - 20 °C
2.1: manganese(IV) oxide / acetone / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 4 h / 0 - 50 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C
With
manganese(IV) oxide; n-butyllithium; carbon dioxide; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2011.01.012
- Guidance literature:
-
Multi-step reaction with 4 steps
1: manganese(IV) oxide / acetone / 20 °C
2: sodium hydride / N,N-dimethyl-formamide / 4 h / 0 - 50 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
4: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C
With
manganese(IV) oxide; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2011.01.012