5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Base Information

Chemical Name:5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside
CAS No.:189144-79-4
Molecular Formula:C₆₂H₈₄O₃₅
Molecular Weight:1389.33
Hs Code.:

5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Synonyms:5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Suppliers and Price of 5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Chemical Property of 5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Technology Process of 5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

There total 8 articles about 5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-2-acetoxymethyl-5-benzyloxy-6-((3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-chloro-tetrahydro-pyran-3-yloxy)-tetrahydro-pyran-4-yl ester

: 189144-70-5
6-[(2S,3R,4S,5R,6R)-4,5-Diacetoxy-6-acetoxymethyl-3-((2R,3R,4R,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-3-hydroxy-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoic acid methyl ester

: 189144-79-4
5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver perchlorate; silver carbonate; In dichloromethane; at 23 ℃; for 30h;
DOI:10.1021/jo962300y

Reference yield:

: 4547-43-7
methyl 6-hydroxycaproate

: 189144-79-4
5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / hex-1-ene, ethyldiisopropylamine / CH₂Cl₂ / 36 h / 23 °C

2: 83 percent / H₂, AcOH / Pd-C / ethanol / 24 h / 23 °C / 10343 Torr

3: 1.) Ag₂CO₃, 4 Angstroem molecular sieves, 2.) AgClO₄ / 1) CH₂Cl₂, 23 deg C, 1 h; 2) CH₂Cl₂, 0 deg C, 80 min

4: 86 percent / H₂, AcOH / Pd-C / ethanol / 24 h / 23 °C / 15514.4 Torr

5: 66 percent / Ag₂CO₃, 4 Angstroem molecular sieves, AgClO₄ / CH₂Cl₂ / 30 h / 23 °C

With 1-hexene; 4 A molecular sieve; hydrogen; silver perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; silver carbonate; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo962300y

Reference yield:

: 173398-22-6
3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl bromide

: 189144-79-4
5-(methoxycarbonyl)pentyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1->2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / hex-1-ene, ethyldiisopropylamine / CH₂Cl₂ / 36 h / 23 °C

2: 83 percent / H₂, AcOH / Pd-C / ethanol / 24 h / 23 °C / 10343 Torr

3: 1.) Ag₂CO₃, 4 Angstroem molecular sieves, 2.) AgClO₄ / 1) CH₂Cl₂, 23 deg C, 1 h; 2) CH₂Cl₂, 0 deg C, 80 min

4: 86 percent / H₂, AcOH / Pd-C / ethanol / 24 h / 23 °C / 15514.4 Torr

5: 66 percent / Ag₂CO₃, 4 Angstroem molecular sieves, AgClO₄ / CH₂Cl₂ / 30 h / 23 °C

With 1-hexene; 4 A molecular sieve; hydrogen; silver perchlorate; acetic acid; N-ethyl-N,N-diisopropylamine; silver carbonate; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo962300y