O-(1,2-Dimethylpropyl) α-phenylselenoacetate

Base Information

• Chemical Name: O-(1,2-Dimethylpropyl) α-phenylselenoacetate
• CAS No.: 128010-26-4
• Molecular Formula: C₁₃H₁₈OSe
• Molecular Weight: 269.245
• Mol file: 128010-26-4.mol

Synonyms:O-(1,2-Dimethylpropyl) α-phenylselenoacetate

Chemical Property of O-(1,2-Dimethylpropyl) α-phenylselenoacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-(1,2-Dimethylpropyl) α-phenylselenoacetate

There total 2 articles about O-(1,2-Dimethylpropyl) α-phenylselenoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

3-methyl-2-butanol (598-75-4) + Se-Phenylethynyl selenoacetate (128010-20-8) → O-(1,2-Dimethylpropyl) α-phenylselenoacetate (128010-26-4)

Guidance literature:

toluene-4-sulfonic acid; In tetrahydrofuran; at 80 ℃;

DOI:10.1246/bcsj.63.835

Reference yield:

phenylacetylene (536-74-3) → O-(1,2-Dimethylpropyl) α-phenylselenoacetate (128010-26-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.a) butyllithium, b) selenium

2: 77 percent / p-toluenesulfonic acid / tetrahydrofuran / 80 °C

With selenium; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran;

DOI:10.1246/bcsj.63.835

upstream raw materials:

3-methyl-2-butanol

Se-Phenylethynyl selenoacetate

phenylacetylene

Refernces