C₁₈H₂₂N₂O₄

Base Information

Chemical Name:C₁₈H₂₂N₂O₄
CAS No.:1424322-89-3
Molecular Formula:C₁₈H₂₂N₂O₄
Molecular Weight:330.384
Hs Code.:

C<sub>18</sub>H<sub>22</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₈H₂₂N₂O₄

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Chemical Property of C₁₈H₂₂N₂O₄

Chemical Property:

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Technology Process of C₁₈H₂₂N₂O₄

There total 5 articles about C₁₈H₂₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₀ClNO₃

: 1424322-89-3
C₁₈H₂₂N₂O₄

Guidance literature:: With hydroxylamine; In tetrahydrofuran; water; at 0 - 5 ℃;
DOI:10.1016/j.bmc.2012.12.001

Reference yield:

: 4942-47-6
(adamant-1-yl)-acetic acid

: 1424322-89-3
C₁₈H₂₂N₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; t-butyl bromide / tetrachloromethane / 2 h / 10 - 20 °C

2: aluminum (III) chloride / 100 - 130 °C / Microwave irradiation

3: nitric acid; trifluoroacetic anhydride; acetic acid / 0 - 5 °C

4: thionyl chloride / N,N-dimethyl-formamide; toluene / 1.5 h / 80 °C

5: hydroxylamine / water; tetrahydrofuran / 0 - 5 °C

With aluminum (III) chloride; thionyl chloride; t-butyl bromide; sulfuric acid; hydroxylamine; nitric acid; acetic acid; trifluoroacetic anhydride; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; toluene; 2: |Friedel-Crafts Alkylation;
DOI:10.1016/j.bmc.2012.12.001

Reference yield:

: 161036-56-2
3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetic acid

: 1424322-89-3
C₁₈H₂₂N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; trifluoroacetic anhydride; acetic acid / 0 - 5 °C

2: thionyl chloride / N,N-dimethyl-formamide; toluene / 1.5 h / 80 °C

3: hydroxylamine / water; tetrahydrofuran / 0 - 5 °C

With thionyl chloride; hydroxylamine; nitric acid; acetic acid; trifluoroacetic anhydride; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2012.12.001