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3-benzylaminosydnone

Base Information
  • Chemical Name:3-benzylaminosydnone
  • CAS No.:120061-12-3
  • Molecular Formula:C9H9N3O2
  • Molecular Weight:191.189
  • Hs Code.:
3-benzylaminosydnone

Synonyms:3-benzylaminosydnone

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Chemical Property of 3-benzylaminosydnone
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Technology Process of 3-benzylaminosydnone

There total 2 articles about 3-benzylaminosydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium tetrahydroborate; In methanol; at 0 ℃; for 1h;
DOI:10.3987/COM-88-4568
Guidance literature:
Multi-step reaction with 2 steps
1: 92 percent / trifluoroacetic anhydride / diethyl ether / 1 h / 0 °C
2: 90 percent / sodium borohydride / methanol / 1 h / 0 °C
With sodium tetrahydroborate; trifluoroacetic anhydride; In methanol; diethyl ether;
DOI:10.3987/COM-88-4568
Guidance literature:
With n-butyllithium; 1.) THF, hexane, <-20 degC, 1 h; 2.) THF, -78 degC -> r.t., overnight;
DOI:10.3987/COM-88-4568
Downstream raw materials:

3-benzylamino-4-benzoylsydnone

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