4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

Base Information

Chemical Name:4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile
CAS No.:1533424-09-7
Molecular Formula:C₁₃H₁₆N₆
Molecular Weight:256.31
Hs Code.:

Synonyms:4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

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Chemical Property of 4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

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Technology Process of 4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

There total 5 articles about 4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1533434-75-1
(Z)-methyl N-(3-tert-butyl-4-cyanophenyl)-N'-cyanocarbamimidothioate

: 1533424-09-7
4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

Guidance literature:: With hydrazine; In ethanol; at 65 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 59255-98-0
2-(tert-butyl)-4-nitroaniline

: 1533424-09-7
4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert.-butylnitrite / dimethyl sulfoxide / 3 h / 60 °C / 760.05 Torr / Inert atmosphere

2.1: iron; ammonium chloride; water / methanol / 60 °C / 760.05 Torr / Inert atmosphere

3.1: calcium carbonate / dichloromethane; water / 0 - 20 °C / 760.05 Torr / Inert atmosphere

4.1: sodium methylate / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

4.2: 1 h / 760.05 Torr / Inert atmosphere

4.3: 20 °C / 760.05 Torr / Inert atmosphere

5.1: hydrazine / ethanol / 65 °C / 760.05 Torr / Inert atmosphere

With tert.-butylnitrite; water; sodium methylate; iron; ammonium chloride; calcium carbonate; hydrazine; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 14034-96-9
2-tert-butyl-4-nitrobenzonitrile

: 1533424-09-7
4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-tert-butylbenzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: iron; ammonium chloride; water / methanol / 60 °C / 760.05 Torr / Inert atmosphere

2.1: calcium carbonate / dichloromethane; water / 0 - 20 °C / 760.05 Torr / Inert atmosphere

3.1: sodium methylate / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

3.2: 1 h / 760.05 Torr / Inert atmosphere

3.3: 20 °C / 760.05 Torr / Inert atmosphere

4.1: hydrazine / ethanol / 65 °C / 760.05 Torr / Inert atmosphere

With water; sodium methylate; iron; ammonium chloride; calcium carbonate; hydrazine; In methanol; ethanol; dichloromethane; water;