C₅₅H₈₃N₅O₅Si₂

Base Information

• Chemical Name: C₅₅H₈₃N₅O₅Si₂
• CAS No.: 1180565-17-6
• Molecular Formula: C₅₅H₈₃N₅O₅Si₂
• Molecular Weight: 950.466
• Mol file: 1180565-17-6.mol

Synonyms:C₅₅H₈₃N₅O₅Si₂

Chemical Property of C₅₅H₈₃N₅O₅Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₈₃N₅O₅Si₂

There total 3 articles about C₅₅H₈₃N₅O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(bis(2-hydroxyethyl)amino)benzaldehyde (27913-86-6) → C55H83N5O5Si2 (1180565-17-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.1: ethanol / 0.5 h / 60 °C / Inert atmosphere

3.1: sodium carbonate / acetonitrile / 70 °C / Inert atmosphere

3.2: 70 °C / Inert atmosphere

With 1H-imidazole; sodium carbonate; In ethanol; N,N-dimethyl-formamide; acetonitrile; 2.1: Knoevenagel condensation;

DOI:10.1007/s10847-010-9781-9

Reference yield:

1-(bromomethyl)-3,5-di(2-ethylhexyloxy)benzene (861889-27-2) + C32H45N5O3Si2 (959738-54-6) → C55H83N5O5Si2 (1180565-17-6)

Guidance literature:

C₃₂H₄₅N₅O₃Si₂; With sodium carbonate; In acetonitrile; at 70 ℃; Inert atmosphere;

1-(bromomethyl)-3,5-di(2-ethylhexyloxy)benzene; In acetonitrile; at 70 ℃; Inert atmosphere;

DOI:10.1007/s10847-010-9781-9

Reference yield:

4-N,N-bis(2-tert-butyldimethylsiloxyethyl)aminobenzaldehyde → C55H83N5O5Si2 (1180565-17-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 0.5 h / 60 °C / Inert atmosphere

2.1: sodium carbonate / acetonitrile / 70 °C / Inert atmosphere

2.2: 70 °C / Inert atmosphere

With sodium carbonate; In ethanol; acetonitrile; 1.1: Knoevenagel condensation;

DOI:10.1007/s10847-010-9781-9

upstream raw materials:

1-(bromomethyl)-3,5-di(2-ethylhexyloxy)benzene

C₃₂H₄₅N₅O₃Si₂

4-(bis(2-hydroxyethyl)amino)benzaldehyde

Downstream raw materials:

C₄₃H₅₅N₅O₅