N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester

Base Information

• Chemical Name: N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester
• CAS No.: 343254-50-2
• Molecular Formula: C₈₄H₈₆NO₂₇P
• Molecular Weight: 1572.57

Synonyms:N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester

Chemical Property of N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester

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Technology Process of N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester

There total 1 articles about N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C100H104NO27PSi → N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester (343254-50-2) + N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl-α-D-galactopyranosyl)-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)]}-L-serine benzyl ester

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; for 10h;

DOI:10.1021/jo001540h

Reference yield:

N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester (343254-50-2) → C84H85NO30PS(1-)*Na(1+)

Guidance literature:

N-benzyloxycarbonyl-O-{O-[(2,3,4-tri-O-4-methylbenzoyl)-β-D-galactopyranosyl]-(1->3)-O-(2-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->4)-(3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranosyl)}-L-serine benzyl ester; With trimethyl-sulfo-ammonium betaine; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 6h;

With AG₅₀W-X₈ (Na⁺); Further stages.;

DOI:10.1021/jo001540h

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