C₃₁H₃₄Br₂N₃O₈P

Base Information

Chemical Name:C₃₁H₃₄Br₂N₃O₈P
CAS No.:1421275-99-1
Molecular Formula:C₃₁H₃₄Br₂N₃O₈P
Molecular Weight:767.408
Hs Code.:

C<sub>31</sub>H<sub>34</sub>Br<sub>2</sub>N<sub>3</sub>O<sub>8</sub>P

Synonyms:C₃₁H₃₄Br₂N₃O₈P

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Chemical Property of C₃₁H₃₄Br₂N₃O₈P

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Technology Process of C₃₁H₃₄Br₂N₃O₈P

There total 3 articles about C₃₁H₃₄Br₂N₃O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1191252-49-9
3-(3,5-dibromo-4-hydroxyphenyl)-N-(4-phenoxybenzyl)-1,2,4-oxadiazole-5-carboxamide

: 229625-50-7
di-tert-butyl chloromethyl phosphate

: 1421275-99-1
C₃₁H₃₄Br₂N₃O₈P

Guidance literature:: 3-(3,5-dibromo-4-hydroxyphenyl)-N-(4-phenoxybenzyl)-1,2,4-oxadiazole-5-carboxamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.75h;

di-tert-butyl chloromethyl phosphate; In N,N-dimethyl-formamide; at 50 ℃;

Reference yield:

: 13086-84-5
di-tert-butyl phosphite

: 1421275-99-1
C₃₁H₃₄Br₂N₃O₈P

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydrogencarbonate; potassium permanganate / water / 1.75 h / 0 - 60 °C

1.2: 0 - 5 °C

2.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate / water; dichloromethane / 0.17 h / 0 °C

2.2: 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C

3.2: 50 °C

With potassium permanganate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; sodium hydrogencarbonate; potassium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 33494-81-4
phosphoric acid di-tert-butyl ester

: 1421275-99-1
C₃₁H₃₄Br₂N₃O₈P

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate / water; dichloromethane / 0.17 h / 0 °C

1.2: 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C

2.2: 50 °C

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; sodium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;