5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Base Information

Chemical Name:5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine
CAS No.:132076-56-3
Molecular Formula:C₃₈H₄₄N₁₀O₂₀P₂
Molecular Weight:1022.77
Hs Code.:

5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-<N-(6-nitroveratryloxycarbonyl)-L-phenylalanyl>adenosine

Synonyms:5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

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Chemical Property of 5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

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Technology Process of 5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

There total 4 articles about 5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 132076-56-3
5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Na₂CO₃ / H₂O; dioxane / 1 h / Ambient temperature

2: 94 percent / Et₃N / 24 h / Ambient temperature

3: 1.) Dowex 1x8-200 ion-exchange beads (Bu₄N-form), Bu₄NOH / 1.) H₂O, 2.) DMF, RT, 2.5 h

With Dowex 1x8-200 ion-exchange beads (Bu₄N-form); tetra(n-butyl)ammonium hydroxide; sodium carbonate; triethylamine; In 1,4-dioxane; water;
DOI:10.1021/ja00007a055

Reference yield:

: 42855-00-5
nitroveratryloxycarbonyl chloride

: 132076-56-3
5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Na₂CO₃ / H₂O; dioxane / 1 h / Ambient temperature

2: 94 percent / Et₃N / 24 h / Ambient temperature

3: 1.) Dowex 1x8-200 ion-exchange beads (Bu₄N-form), Bu₄NOH / 1.) H₂O, 2.) DMF, RT, 2.5 h

With Dowex 1x8-200 ion-exchange beads (Bu₄N-form); tetra(n-butyl)ammonium hydroxide; sodium carbonate; triethylamine; In 1,4-dioxane; water;
DOI:10.1021/ja00007a055

Reference yield:

: 30034-25-4
N-(4,5-dimethoxy-2-nitrobenzyloxycarbonyl)-L-phenylalanine

: 132076-56-3
5'-phospho-2'-deoxycytidylyl(3'-5')-2'-O-adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Et₃N / 24 h / Ambient temperature

2: 1.) Dowex 1x8-200 ion-exchange beads (Bu₄N-form), Bu₄NOH / 1.) H₂O, 2.) DMF, RT, 2.5 h

With Dowex 1x8-200 ion-exchange beads (Bu₄N-form); tetra(n-butyl)ammonium hydroxide; triethylamine;
DOI:10.1021/ja00007a055