1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

Base Information

Chemical Name:1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene
CAS No.:1354640-68-8
Molecular Formula:C₂₄H₂₇BrO₄
Molecular Weight:459.38
Hs Code.:

Synonyms:1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

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Technology Process of 1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

There total 4 articles about 1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 54370-00-2
2-bromo-4,5-dimethoxybenzyl alcohol

: 104581-29-5
1-[2-(4-methoxyphenyl)ethynyl]cyclohexanol

: 1354640-68-8
1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

Guidance literature:: With copper(ll) bromide; In acetonitrile; at 20 ℃;
DOI:10.1055/s-0031-1289545

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 1354640-68-8
1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol

2: copper(ll) bromide / acetonitrile / 20 °C

With sodium tetrahydroborate; copper(ll) bromide; In methanol; acetonitrile;
DOI:10.1055/s-0031-1289545

Reference yield:

: 696-62-8
para-iodoanisole

: 1354640-68-8
1-((1-(2-(4-methoxyphenyl)ethynyl)cyclohexyloxy)methyl)-2-bromo-4,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine

2: copper(ll) bromide / acetonitrile / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; copper(ll) bromide; In acetonitrile; 1: Sonogashira coupling;
DOI:10.1055/s-0031-1289545