N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

Base Information

Chemical Name:N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate
CAS No.:218603-30-6
Molecular Formula:C₂₂H₂₅N₅O₇
Molecular Weight:471.47
Hs Code.:

N-<4-<N-(6-<<(aminocarbonyl)amino>carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

Synonyms:N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

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Chemical Property of N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

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Technology Process of N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

There total 8 articles about N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 52407-60-0
dimethyl N-(4-amino-benzoyl)-L-glutamate

: 218603-23-7
N-(6-formylpyridin-2-ylcarbonyl)urea

: 218603-30-6
N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

Guidance literature:: With 3 A molecular sieve; sodium cyanoborohydride; trifluoroacetic acid; In dichloromethane; for 120h;

Reference yield:

: 5453-67-8
2,6-bis(methoxycarbonyl)pyridine

: 218603-30-6
N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / DIBAL-H / CH₂Cl₂ / 3 h / -78 °C

2: 98 percent / pyridinium toluene-p-sulphonate / methanol

3: 1.) KH / 1.) THF, 4 h, 2.) THF, 1.5 h

4: 78 percent / 15 percent aq. H₂SO₄ / CH₂Cl₂ / 6 h / Ambient temperature

5: 57 percent / NaBH₃CN, TFA, molecular sieves 3A / CH₂Cl₂ / 120 h

With 3 A molecular sieve; sulfuric acid; pyridinium p-toluenesulfonate; potassium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; trifluoroacetic acid; In methanol; dichloromethane;

Reference yield:

: 69950-65-8
methyl 6-formylpicolinate

: 218603-30-6
N-<4-carbonyl>pyridin-2-ylmethyl)>aminobenzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / pyridinium toluene-p-sulphonate / methanol

2: 1.) KH / 1.) THF, 4 h, 2.) THF, 1.5 h

3: 78 percent / 15 percent aq. H₂SO₄ / CH₂Cl₂ / 6 h / Ambient temperature

4: 57 percent / NaBH₃CN, TFA, molecular sieves 3A / CH₂Cl₂ / 120 h

With 3 A molecular sieve; sulfuric acid; pyridinium p-toluenesulfonate; potassium hydride; sodium cyanoborohydride; trifluoroacetic acid; In methanol; dichloromethane;