6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

Base Information

Chemical Name:6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one
CAS No.:1207624-05-2
Molecular Formula:C₁₂H₁₂BrN₃O
Molecular Weight:294.151
Hs Code.:

Synonyms:6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

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Chemical Property of 6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

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Technology Process of 6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

There total 1 articles about 6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38875-53-5
5-bromo-pyridine-2,3-diamine

: 1655-07-8
ethyl 2-oxocyclohexane carboxylate

: 1207624-05-2
6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

Guidance literature:: In xylene; for 64h; Reflux;

Reference yield:

: 14774-37-9
(tetrahydro-2H-pyran-4-yl)methanol

: 1207624-05-2
6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

: 1207624-06-3
6-Bromo-3-cyclohex-1-en-1-yl-1-(tetrahydro-2H-pyran-4-ylmethyl)-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield:

: 1207624-05-2
6-Bromo-3-cyclohex-1-en-1-yl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

: 1207624-07-4
3-cyclohex-1-en-1-yl-1-(tetrahydro-2H-pyran-4-ylmethyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaboran-2-yl)-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 6.5 h / 80 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; potassium acetate; triphenylphosphine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; N,N-dimethyl-formamide;