(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

Base Information

Chemical Name:(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester
CAS No.:97592-05-7
Molecular Formula:C₁₈H₂₃BrO₄
Molecular Weight:383.282
Hs Code.:

Synonyms:(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

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Chemical Property of (Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

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Technology Process of (Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

There total 4 articles about (Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 87102-06-5
6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

: 97592-05-7
(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

Guidance literature:: With N-Bromosuccinimide; dimethylsulfide; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1021/jo00220a034

Reference yield:

: 87102-03-2
3-formylpropyl 2,4,6-trimethyl benzoate

: 97592-05-7
(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DABCO / 168 h / Ambient temperature

2: 89 percent / N-bromosuccinimide, Me₂S / CH₂Cl₂ / 16 h / Ambient temperature

With 1,4-diaza-bicyclo[2.2.2]octane; N-Bromosuccinimide; dimethylsulfide; In dichloromethane;
DOI:10.1021/jo00220a034

Reference yield:

: 97592-16-0
4-hydroxybutyl 2,4,6-trimethylbenzoate

: 97592-05-7
(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(bromomethyl)-2-hexanoic acid, methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / pyridine chlorochromate / CH₂Cl₂ / 2 h

2: 87 percent / DABCO / 168 h / Ambient temperature

3: 89 percent / N-bromosuccinimide, Me₂S / CH₂Cl₂ / 16 h / Ambient temperature

With 1,4-diaza-bicyclo[2.2.2]octane; N-Bromosuccinimide; dimethylsulfide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jo00220a034