2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine

Base Information

• Chemical Name: 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine
• CAS No.: 1228585-17-8
• Molecular Formula: C₃₇H₂₃Cl₂N₃
• Molecular Weight: 580.516
• Mol file: 1228585-17-8.mol

Synonyms:2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine

Chemical Property of 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine

There total 2 articles about 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-oxadiazin-1-ium hexachloroantimonic acid → 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine (1228585-17-8)

Guidance literature:

With ammonium hydroxide; In water; at 0 - 20 ℃; for 1h;

Reference yield:

5-chlorobiphenyl-3-carbonitrile (1214363-96-8) + 2-naphthaloyl chloride (2243-83-6) → 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine (1228585-17-8)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform / 7 h / 0 °C / Reflux

2: ammonium hydroxide / water / 1 h / 0 - 20 °C

With ammonium hydroxide; In chloroform; water;

Reference yield: 95.0%

(4-(pyridin-2-yl)phenyl)boronic acid (170230-27-0) + 2,4-bis(5-chlorobiphenyl-3-yl)-6-(2-naphthyl)-1,3,5-triazine (1228585-17-8) → 2-(2-naphthyl)-4,6-bis[4-(2-pyridyl)-1,1':3',1'-terphenyl-5'-yl]-1,3,5-triazine (1228585-30-5)

Guidance literature:

With caesium carbonate; palladium diacetate; XPhos; In tetrahydrofuran; for 22h; Inert atmosphere; Reflux;

upstream raw materials:

5-chlorobiphenyl-3-carbonitrile

2-naphthaloyl chloride

Downstream raw materials:

2-(2-naphthyl)-4,6-bis[4-(2-pyridyl)-1,1':3',1'-terphenyl-5'-yl]-1,3,5-triazine