Technology Process of C26H19ClO2
There total 3 articles about C26H19ClO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate;
In
tetrahydrofuran;
at 50 ℃;
for 22h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ol200676k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 22 h / 20 °C / Inert atmosphere
2: 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate / tetrahydrofuran / 22 h / 50 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water;
1: Suzuki-Miyaura coupling / 2: Suzuki-Miyaura coupling;
DOI:10.1021/ol200676k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 22 h / 20 °C / Inert atmosphere
3: 1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; palladium diacetate / tetrahydrofuran / 22 h / 50 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate;
In
tetrahydrofuran; water;
1: Suzuki-Miyaura coupling / 2: Suzuki-Miyaura coupling / 3: Suzuki-Miyaura coupling;
DOI:10.1021/ol200676k
