ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

Base Information

Chemical Name:ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate
CAS No.:1359937-93-1
Molecular Formula:C₂₅H₃₀N₄O₅S
Molecular Weight:498.603
Hs Code.:

Synonyms:ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

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Chemical Property of ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

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Technology Process of ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

There total 4 articles about ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1359937-94-2
ethyl 6-(2-aminoethoxy)-1-benzyl-2,3-dihydro-1H-inden-2-ylcarbamate

: 137049-00-4
1-methyl-1H-imidazole-4-sulfonyl chloride

: 1359937-93-1
ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; Product distribution / selectivity;

Reference yield:

: ethyl 1-benzyl-6-hydroxy-2,3-dihydro-1H-indene-2-ylcarbamate

: 1359937-93-1
ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / acetonitrile / 1 h / 80 °C / Inert atmosphere

1.2: 2 h / 50 - 80 °C

2.1: formic acid / 20 °C

3.1: dmap / dichloromethane / 20 °C

With dmap; formic acid; caesium carbonate; In dichloromethane; acetonitrile;

Reference yield:

: cis-ethyl 1-benzyl-6-methoxy-2,3-dihydro-1H-inden-2-ylcarbamate

: 1359937-93-1
ethyl 1-benzyl-6-(2-(1-methyl-1H-imidazole-4-sulfonamido)ethoxy)-2,3-dihydro-1H-inden-2-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / Inert atmosphere

1.2: Cooling with ice

2.1: caesium carbonate / acetonitrile / 1 h / 80 °C / Inert atmosphere

2.2: 2 h / 50 - 80 °C

3.1: formic acid / 20 °C

4.1: dmap / dichloromethane / 20 °C

With dmap; formic acid; boron tribromide; caesium carbonate; In dichloromethane; acetonitrile;