N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide

Base Information

Chemical Name:N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide
CAS No.:1428555-91-2
Molecular Formula:C₁₂H₁₆N₂O
Molecular Weight:204.272
Hs Code.:

Synonyms:N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide

Chemical Property:

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Technology Process of N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide

There total 2 articles about N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50675-57-5,89312-77-6,103554-20-7
dl-2,2-dimethylcyclopropane-1-carboxylic acid chloride

: 95-54-5
1,2-diamino-benzene

: 1428555-91-2
N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide

: 1428555-92-3
1,2-bis(2,2-dimethylcyclopropyl-1-carbonylamino)benzene

Guidance literature:: With triethylamine; In acetonitrile; at -25 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2013.02.021

Reference yield:

: 75885-59-5,931-26-0
2,2-dimethylcyclopropane-1-carboxylic acid

: 1428555-91-2
N-(2-aminophenyl)-2,2-dimethylcyclopropanecarboxamide

: 1428555-92-3
1,2-bis(2,2-dimethylcyclopropyl-1-carbonylamino)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride; pyridine / diethyl ether / 1 h / 20 °C

2: triethylamine / acetonitrile / 2 h / -25 - 20 °C

3: acetic acid / 3 h / Reflux

4: 0.5 h / 202 °C

With pyridine; thionyl chloride; triethylamine; In diethyl ether; acetic acid; acetonitrile;
DOI:10.1016/j.tet.2013.02.021