Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

Base Information

Chemical Name:Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside
CAS No.:164322-54-7
Molecular Formula:C₂₂H₂₃F₃O₈S
Molecular Weight:504.481
Hs Code.:

Synonyms:Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

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Technology Process of Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

There total 2 articles about Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 15038-71-8,15384-58-4,23392-29-2,40653-23-4,57539-07-8,76375-66-1,78185-83-8,81872-62-0,86363-45-3,90639-38-6,108739-91-9,116002-34-7,130192-76-6,131433-04-0,141115-75-5
methyl 2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: 358-23-6
trifluoromethylsulfonic anhydride

: 164322-54-7
Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at -20 ℃; for 2h;
DOI:10.1080/07328309608005695

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 76375-66-1
methyl 2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: 164322-54-7
Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo00119a011

Reference yield:

: 164322-54-7
Methyl 2-O-benzyl-4,6-O-benzylidene-3-O-<(trifluoromethyl)sulfonyl>-α-D-glucopyranoside

: (1S,3S,4R,5R,6R)-4-benzyloxy-6-hydroxy-3-methoxy-2,7-dioxabicyclo[3.3.0]octane

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; 1,1,1,3',3',3'-hexafluoro-propanol; water; In dichloromethane; for 1.5h; Yield given; Heating;
DOI:10.1021/jo00119a011