2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

Base Information

Chemical Name:2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine
CAS No.:1268250-72-1
Molecular Formula:C₄₄H₃₀N₄
Molecular Weight:614.749
Hs Code.:

Synonyms:2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

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Chemical Property of 2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

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Technology Process of 2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

There total 2 articles about 2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 129013-83-8
3-(4-bromophenyl)pyridine

: 1268250-71-0
2-[3,5-bis(4,4,5,5-tetrarmethyl-1,3,2-dioxaborolan-2-yl)phenyl]-4,6-diphenylpyrimidine

: 1268250-72-1
2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

Guidance literature:: With caesium carbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 12h; Inert atmosphere; Reflux;

Reference yield:

: 942132-67-4
2-(3,5-dibromophenyl)-4,6-diphenylpyrimidine

: 1268250-72-1
2-[4,4''-di(3-pyridyl)-1,1':3',1''-terphenyl-5'-yl]-4,6-diphenylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 77 h / Inert atmosphere; Reflux

2: caesium carbonate / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux

With potassium acetate; caesium carbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran;