5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

Base Information

Chemical Name:5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole
CAS No.:174153-41-4
Molecular Formula:C₁₇H₂₄N₂O₂Si
Molecular Weight:316.475
Hs Code.:

Synonyms:5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

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Chemical Property of 5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

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Technology Process of 5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

There total 1 articles about 5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 154876-20-7
1-hydrazinecarboxylic acid 2-(trimethylsilyl)ethyl ester

: 583-05-1
1-phenylpentane-1,4-dione

: 174153-41-4
5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

Guidance literature:: With pyridinium p-toluenesulfonate; In toluene; at 60 ℃; for 10h;
DOI:10.1021/jo9518260

Reference yield: 62.0%

: 174153-41-4
5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

: 3042-24-8
2-methyl-5-phenyl-1H-pyrrol-1-amine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 5h; Ambient temperature;
DOI:10.1021/jo9518260

Reference yield:

: 174153-41-4
5-methyl-2-phenyl-1-<<<<2-(trimethylsilyl)ethyl>oxy>carbonyl>amino>pyrrole

: 1-(5-methyl-2-phenyl-1-pyrrolyl)-2,5-diphenylpyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / nBu₄NF / tetrahydrofuran / 5 h / Ambient temperature

2: 88 percent / p-toluenesulfonic acid / toluene / 5 h / 60 °C

With tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1021/jo9518260