Carbamic acid, diethyl-, 3,4-dichlorophenyl ester

Base Information

Chemical Name:Carbamic acid, diethyl-, 3,4-dichlorophenyl ester
CAS No.:204930-39-2
Molecular Formula:C₁₁H₁₃Cl₂NO₂
Molecular Weight:262.136
Hs Code.:
DSSTox Substance ID:DTXSID501235241

Synonyms:Carbamic acid, diethyl-, 3,4-dichlorophenyl ester;SCHEMBL23214505;DTXSID501235241;204930-39-2

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Chemical Property of Carbamic acid, diethyl-, 3,4-dichlorophenyl ester

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:261.0323340
Heavy Atom Count:16
Complexity:234

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)C(=O)OC1=CC(=C(C=C1)Cl)Cl

Technology Process of Carbamic acid, diethyl-, 3,4-dichlorophenyl ester

There total 1 articles about Carbamic acid, diethyl-, 3,4-dichlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 95-77-2
3,4-dichlorophenol

: 88-10-8
N,N-diethylcarbamyl chloride

: 204930-39-2
O-3,4-dichlorophenyl N,N-diethylcarbamate

Guidance literature:: With pyridine; at 100 ℃;
DOI:10.1016/S0040-4020(98)83030-5

Reference yield: 80.0%

: 204930-39-2
O-3,4-dichlorophenyl N,N-diethylcarbamate

: O-3,4-dichloro-2-deuteriophenyl N,N-diethylcarbamate

Guidance literature:: O-3,4-dichlorophenyl N,N-diethylcarbamate; With sec.-butyllithium; In tetrahydrofuran; at -78 - -65 ℃; for 1.58333h; Inert atmosphere;

With d⁽⁴⁾-methanol; In tetrahydrofuran; at -65 ℃; for 0.25h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201600933