7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

Base Information

Chemical Name:7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside
CAS No.:904684-06-6
Molecular Formula:C₅₀H₄₈O₁₇
Molecular Weight:920.921
Hs Code.:

Synonyms:7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

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Chemical Property of 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

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Technology Process of 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

There total 1 articles about 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 904684-05-5
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-β-D-xylopyranoside

: 108-24-7
acetic anhydride

: 904684-06-6
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

: 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-2-O-acetyl-β-D-xylopyranoside

Guidance literature:: 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-β-D-xylopyranoside; With di(n-butyl)tin oxide; In 1,4-dioxane; benzene; for 6h; Heating;

acetic anhydride; In benzene; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2006.02.011

Reference yield:

: 904684-06-6
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

: 904684-09-9
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 1 h

2: 724 mg / m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / -10 °C

3: 93 percent / hydrazine hydrate; acetic acid / pyridine / 0.13 h / 20 °C

With 1H-tetrazole; hydrazine hydrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2006.02.011

Reference yield:

: 904684-06-6
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

: 904684-08-8
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 1 h

2: 724 mg / m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / -10 °C

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2006.02.011