chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride

Base Information

Chemical Name:chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride
CAS No.:73509-67-8
Molecular Formula:C₂₅H₂₀ClO₂PRe*Cl
Molecular Weight:640.519
Hs Code.:

Synonyms:chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride

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Technology Process of chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride

There total 1 articles about chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (η5-C5H5)Re(CO)2(PPh3)

: 73509-67-8
chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride

Guidance literature:: With Cl₂; In tetrachloromethane; under argon; Cl2 bubbled at -15 to -10°C for 1 h; ppt. filtered off, washed (CCl4), dried at -10°C in an Ar stream; elem. anal.;
DOI:10.1007/BF00953593

Reference yield: 99.0%

: 13826-83-0
ammonium tetrafluroborate

: 73509-67-8
chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium chloride

: 78295-35-9
chloro-π-cyclopentadienyl(triphenylphosphine)dicarbonylrhenium tetrafluoroborate

Guidance literature:: With SOCl₂; In water; under argon; mixed with stirring; ppt. filtered off, washed (water), dried (P2O5); elem. anal.;
DOI:10.1007/BF00953593