2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

Base Information

Chemical Name:2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate
CAS No.:1636872-35-9
Molecular Formula:C₂₆H₂₆N₂O₃S₂
Molecular Weight:478.636
Hs Code.:

Synonyms:2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

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Chemical Property of 2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

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Technology Process of 2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

There total 4 articles about 2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 873-58-5
sodium N-morpholinocarbamodithioate

: 1636871-91-4
1?(α?chloroacetyl)?(3E,5E)?3,5?bis(benzylidene)?piperidin?4?one

: 1636872-35-9
2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

Guidance literature:: In methanol; water; at 60 ℃;
DOI:10.1039/c4ra03655g

Reference yield:

: 132766-61-1,145888-81-9
3,5-dibenzylidenepiperidin-4-one

: 1636872-35-9
2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane / 3 h / 0 - 20 °C

2: water; methanol / 60 °C

With potassium carbonate; In methanol; dichloromethane; water;
DOI:10.1039/c4ra03655g

Reference yield:

: 41979-39-9
4-piperidone hydrochloride

: 1636872-35-9
2-((3E,5E)-3,5-dibenzylidene-4-oxopiperidin-1-yl)-2-oxoethyl morpholine-4-carbodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 3 h / 20 °C

2: potassium carbonate / dichloromethane / 3 h / 0 - 20 °C

3: water; methanol / 60 °C

With potassium carbonate; sodium hydroxide; In methanol; dichloromethane; water; 1: |Aldol Condensation;
DOI:10.1039/c4ra03655g