2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol

Base Information

• Chemical Name: 2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol
• CAS No.: 129165-96-4
• Molecular Formula: C₂₁H₁₂N₄O₄S₂
• Molecular Weight: 448.483

Synonyms:2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol

Chemical Property of 2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol

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Technology Process of 2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol

There total 1 articles about 2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(Dimethyldithiocarbamate)-6-<(p-nitrophenyl)thio>benzthiazol (129165-93-1) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) → 2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol (129165-96-4)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; for 5h; Heating;

Reference yield: 79.0%

2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol (129165-96-4) + 4-chloro-aniline (106-47-8) → 3-(4-Chloro-phenyl)-2-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-ylamino]-3H-quinazolin-4-one (129166-02-5)

Guidance literature:

at 155 - 160 ℃; for 0.5h;

Reference yield: 77.0%

2-(4H-3,1-Benzoxazin-4-on-2-yl)imino-6-<(p-nitrophenyl)thio>benzthiazol (129165-96-4) + p-toluidine (106-49-0,12221-03-3) → 2-[6-(4-Nitro-phenylsulfanyl)-benzothiazol-2-ylamino]-3-p-tolyl-3H-quinazolin-4-one (129166-03-6)

Guidance literature:

at 155 - 160 ℃; for 0.5h;

upstream raw materials:

2-(Dimethyldithiocarbamate)-6-<(p-nitrophenyl)thio>benzthiazol

anthranilic acid

Downstream raw materials:

2-<(4H-3,1-Benzoxazin-4-one-2-yl)imino>-6-<(p-nitrophenyl)thio>benzthiazol

2-[6-(4-Nitro-phenylsulfanyl)-benzothiazol-2-ylamino]-3-p-tolyl-3H-quinazolin-4-one

3-(4-Chloro-phenyl)-2-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-ylamino]-3H-quinazolin-4-one

3-(4-Methoxy-phenyl)-2-[6-(4-nitro-phenylsulfanyl)-benzothiazol-2-ylamino]-3H-quinazolin-4-one

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