(2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

Base Information

Chemical Name:(2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester
CAS No.:415678-77-2
Molecular Formula:C₁₈H₂₄N₂O₄
Molecular Weight:332.4
Hs Code.:

Synonyms:(2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

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Chemical Property of (2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

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Technology Process of (2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

There total 4 articles about (2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 415678-68-1
(2,4-dimethyl-3-pentyl) γ-benzyloxyacetoacetate

: 415678-77-2
(2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

Guidance literature:: With triethylamine; Methanesulfonyl azide; In acetonitrile; at 20 ℃;
DOI:10.1021/ol010283f

Reference yield:

: 17790-81-7
methyl 4-bromo-3-oxobutanoate

: 415678-77-2
(2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / NaH / hexane; tetrahydrofuran / 20 °C

2: 76 percent / DMAP / toluene / Heating

3: 83 percent / MsN₃; NEt₃ / acetonitrile / 20 °C

With dmap; sodium hydride; triethylamine; Methanesulfonyl azide; In tetrahydrofuran; hexane; toluene; acetonitrile;
DOI:10.1021/ol010283f

Reference yield:

: 82961-76-0
4-benzyloxy-3-oxobutyric acid methyl ester

: 415678-77-2
(2,4-dimethyl-3-pentyl) γ-benzyloxy-α-diazo-β-ketoester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / DMAP / toluene / Heating

2: 83 percent / MsN₃; NEt₃ / acetonitrile / 20 °C

With dmap; triethylamine; Methanesulfonyl azide; In toluene; acetonitrile;
DOI:10.1021/ol010283f