(2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole

Base Information

Chemical Name:(2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole
CAS No.:33119-82-3
Molecular Formula:C14H10 Cl N3 S
Molecular Weight:287.7673
Hs Code.:
NSC Number:45090
DSSTox Substance ID:DTXSID90430074
ChEMBL ID:CHEMBL3325578

Synonyms:STK638329;33119-82-3;NSC45090;CHEMBL3325578;DTXSID90430074;NSC-45090;AKOS003652682;AKOS005569859;(2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole

Suppliers and Price of (2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:439°Cat760mmHg
Flash Point:219.3°C
Density:1.36g/cm³
XLogP3:5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:287.0283962
Heavy Atom Count:19
Complexity:318

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)N=C(S2)NN=CC3=CC=C(C=C3)Cl
Isomeric SMILES:C1=CC=C2C(=C1)N=C(S2)N/N=C/C3=CC=C(C=C3)Cl

Technology Process of (2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole

There total 3 articles about (2Z)-2-[(2E)-(4-chlorobenzylidene)hydrazinylidene]-2,3-dihydro-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 104-88-1
4-chlorobenzaldehyde

: 615-21-4
1,3-benzothiazol-2-ylhydrazine

: 33119-82-3
4-cholorobenzaldehyde 2-(2-benzothiazolyl)hydrazone

Guidance literature:: In methanol; at 20 ℃; for 0.5h;
DOI:10.1002/cjoc.201700390

Reference yield: 82.0%

: 104-88-1
4-chlorobenzaldehyde

: 615-21-4
1,3-benzothiazol-2-ylhydrazine

: 33119-82-3
(E)-2-(2-(4-chlorobenzylidene)hydrazinyl)benzo[d]thiazole

Guidance literature:: In ethanol; at 20 ℃;
DOI:10.2174/157018010792062740

Reference yield:

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 33119-82-3
4-cholorobenzaldehyde 2-(2-benzothiazolyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / 4 h / 100 °C

2: acetic acid / ethanol / 4 h / Reflux

With hydrazine hydrate; acetic acid; In ethanol;