(E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

Base Information

Chemical Name:(E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride
CAS No.:96306-68-2
Molecular Formula:C₁₈H₁₈N₂O*ClH
Molecular Weight:314.815
Hs Code.:

Synonyms:(E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

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Technology Process of (E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

There total 4 articles about (E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 96326-01-1
(E)-rac-4,5-dihydro-2-<2-phenyl-2-<4-(phenylmethoxy)phenyl>cyclopropyl>-1H-imidazole

: 96306-68-2
(E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

Guidance literature:: With hydrogenchloride; palladium on activated charcoal; In cyclohexene; for 3h; Heating;
DOI:10.1021/jo00213a004

Reference yield:

: 54589-41-2
(4-(benzyloxy)phenyl)(phenyl)methanone

: 96306-68-2
(E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / H₂NNH₂*H₂O / ethanol / 18 h / Heating

2: 1.) MnO₂ / 1.) CH₂Cl₂, 3 h, 2.) heptane, reflux, 3 h

3: 8 h / 190 °C

4: 94 percent / 3.9 M ethanolic HCl / 10percent Pd/C / cyclohexene / 3 h / Heating

With hydrogenchloride; manganese(IV) oxide; hydrazine hydrate; palladium on activated charcoal; In ethanol; cyclohexene;
DOI:10.1021/jo00213a004

Reference yield:

: 96306-55-7
phenyl<4-(phenylmethoxy)phenyl>methanone hydrazone

: 96306-68-2
(E)-rac-4-<2-(4,5-dihydro-1H-imidazol-2-yl)-1-phenylcyclopropyl>phenol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) MnO₂ / 1.) CH₂Cl₂, 3 h, 2.) heptane, reflux, 3 h

2: 8 h / 190 °C

3: 94 percent / 3.9 M ethanolic HCl / 10percent Pd/C / cyclohexene / 3 h / Heating

With hydrogenchloride; manganese(IV) oxide; palladium on activated charcoal; In cyclohexene;
DOI:10.1021/jo00213a004