2-Bromo-3-methylquinoline

Base Information

Chemical Name:2-Bromo-3-methylquinoline
CAS No.:35740-86-4
Molecular Formula:C10H8 Br N
Molecular Weight:222.08122
Hs Code.:2933499090
DSSTox Substance ID:DTXSID20361246
Nikkaji Number:J3.542.176I
Wikidata:Q82143495
ChEMBL ID:CHEMBL1472106
Mol file:35740-86-4.mol

Synonyms:2-bromo-3-methylquinoline;35740-86-4;HMS2530N21;methyl-bromoquinoline;PROPYLISOVALERATE;AC-907/34107036;MLS000702577;SCHEMBL4161475;CHEMBL1472106;DTXSID20361246;MFCD03695835;AKOS012531976;SB70210;AS-43803;SMR000224608;CS-0312157;FT-0756819;J3.542.176I;EN300-104076;A905799;J-508237;Z1101437829

Suppliers and Price of 2-Bromo-3-methylquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-bromo-3-methylquinoline
50mg
$ 175.00

TRC
2-bromo-3-methylquinoline
100mg
$ 285.00

SynQuest Laboratories
2-Bromo-3-methylquinoline
1 g
$ 632.00

SynQuest Laboratories
2-Bromo-3-methylquinoline
250 mg
$ 216.00

Matrix Scientific
2-Bromo-3-methylquinoline
5g
$ 3353.00

Matrix Scientific
2-Bromo-3-methylquinoline
1g
$ 1118.00

Matrix Scientific
2-Bromo-3-methylquinoline
500mg
$ 720.00

Crysdot
2-Bromo-3-methylquinoline 95+%
1g
$ 672.00

Chemenu
2-bromo-3-methylquinoline 95%
1g
$ 635.00

Apolloscientific
2-Bromo-3-methylquinoline
250mg
$ 196.00

Total 12 raw suppliers

Chemical Property of 2-Bromo-3-methylquinoline

Chemical Property:

Vapor Pressure:0.0011mmHg at 25°C
Refractive Index:1.654
Boiling Point:310.4°Cat760mmHg
Flash Point:141.5°C
PSA：12.89000
Density:1.488g/cm³
LogP:3.30570
Storage Temp.:2-8°C
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:220.98401
Heavy Atom Count:12
Complexity:160

Purity/Quality:

97% ^*data from raw suppliers

2-bromo-3-methylquinoline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=CC=CC=C2N=C1Br

Technology Process of 2-Bromo-3-methylquinoline

There total 4 articles about 2-Bromo-3-methylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1873-55-8
3-methylquinoline N-oxide

: 35740-86-4
2-bromo-3-methylquinoline

Guidance literature:: With N,N-dimethyl-formamide; phosphorus(V) oxybromide; In dichloromethane; at 0 - 25 ℃; for 6h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2016.07.083

Reference yield: 45.0%

: 55539-83-8
1,3-dimethylquinolin-2-(1H)-one

: 35740-86-4
2-bromo-3-methylquinoline

Guidance literature:: With dibromoisocyanuric acid; triphenylphosphine; In neat (no solvent); at 130 - 140 ℃; for 15h; Inert atmosphere;
DOI:10.3987/COM-15-13234

Reference yield:

: 612-58-8
3-methylquinoline

: 35740-86-4
2-bromo-3-methylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,4-dioxane / 2 h / Reflux

1.2: 20 h / 20 °C

2.1: triphenylphosphine; dibromoisocyanuric acid / neat (no solvent) / 15 h / 130 - 140 °C / Inert atmosphere

With dibromoisocyanuric acid; triphenylphosphine; In 1,4-dioxane;
DOI:10.3987/COM-15-13234