N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide

Base Information

• Chemical Name: N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide
• CAS No.: 475469-58-0
• Molecular Formula: C₃₄H₄₀N₂O₈
• Molecular Weight: 604.7
• Mol file: 475469-58-0.mol

Synonyms:N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide

Chemical Property of N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide

There total 1 articles about N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2-(allyloxy)ethyl 4-methylbenzenesulfonate (50563-72-9) + N,N'-bis-[2-(4-hydroxy-phenoxy)-ethyl]-isophthalamide (394219-89-7) → N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide (475469-58-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 16h;

DOI:10.1021/ja027519a

Reference yield: 47.0%

N,N'-bis-{2-[4-(2-allyloxy-ethoxy)-phenoxy]-ethyl}-isophthalamide (475469-58-0) + 3,5-bis-{4-[bis-(4-tert-butyl-phenyl)-phenyl-methyl]-phenylcarbamoyl}-1-methyl-pyridinium; chloride → C74H78N3O2(1+)*C32H36N2O8*Cl(1-)

Guidance literature:

With Grubbs catalyst first generation; In dichloromethane; for 16h;

DOI:10.1021/ja027519a

upstream raw materials:

2-(allyloxy)ethyl 4-methylbenzenesulfonate

N,N'-bis-[2-(4-hydroxy-phenoxy)-ethyl]-isophthalamide