2,3-Difluoro-4-methylanisole

Base Information

Chemical Name:2,3-Difluoro-4-methylanisole
CAS No.:261763-32-0
Molecular Formula:C8H8 F2 O
Molecular Weight:158.148
Hs Code.:2909309090
European Community (EC) Number:670-747-0
DSSTox Substance ID:DTXSID30378901
Wikidata:Q82168488
Mol file:261763-32-0.mol

Synonyms:2,3-Difluoro-4-methylanisole;2,3-difluoro-1-methoxy-4-methylbenzene;261763-32-0;Benzene, 2,3-difluoro-1-methoxy-4-methyl-;SCHEMBL3769995;DTXSID30378901;FKLVEWBHEMLCBM-UHFFFAOYSA-N;MFCD01631321;AKOS006229791;JS-4158;2,3-Difluoro-1-methoxy-4-methyl-benzene;CS-0191795;FT-0691372;A818283

Suppliers and Price of 2,3-Difluoro-4-methylanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
2,3-Difluoro-4-methylanisole
5 g
$ 212.00

SynQuest Laboratories
2,3-Difluoro-4-methylanisole
10 g
$ 386.00

Oakwood
2,3-Difluoro-4-methylanisole
250mg
$ 19.00

Matrix Scientific
2,3-Difluoro-4-methylanisole
1g
$ 25.00

Matrix Scientific
2,3-Difluoro-4-methylanisole
5g
$ 102.00

Crysdot
2,3-Difluoro-1-methoxy-4-methylbenzene 95+%
100g
$ 558.00

AOBChem
2,3-Difluoro-1-methoxy-4-methylbenzene 95%
25g
$ 385.00

American Custom Chemicals Corporation
2,3-DIFLUORO-4-METHYLANISOLE 95.00%
5G
$ 862.79

American Custom Chemicals Corporation
2,3-DIFLUORO-4-METHYLANISOLE 95.00%
1G
$ 604.07

Alichem
2,3-Difluoro-4-methylanisole
1g
$ 1519.80

Total 11 raw suppliers

Chemical Property of 2,3-Difluoro-4-methylanisole

Chemical Property:

Boiling Point:172.9±35.0 °C(Predicted)
Density:1.144±0.06 g/cm3(Predicted)
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:158.05432120
Heavy Atom Count:11
Complexity:129

Purity/Quality:

97% ^*data from raw suppliers

2,3-Difluoro-4-methylanisole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)OC)F)F

Technology Process of 2,3-Difluoro-4-methylanisole

There total 1 articles about 2,3-Difluoro-4-methylanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 261763-45-5
2,3-difluoro-4-methylphenol

: 77-78-1
dimethyl sulfate

: 261763-32-0
2,3-difluoro-1-methoxy-4-methylbenzene

Guidance literature:: With sodium hydroxide; In water; at 20 ℃;

Reference yield: 61.0%

: 261763-32-0
2,3-difluoro-1-methoxy-4-methylbenzene

: 689254-23-7
1-(bromomethyl)-2,3-difluoro-4-methoxybenzene

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 3.5h; Heating / reflux;

Reference yield:

: 261763-32-0
2,3-difluoro-1-methoxy-4-methylbenzene

: 1'-(1-methylethyl)-4'-[(2,3-difluoro-4-methoxyphenyl)methyl]-5'-methyl-1H-pyrazol-3'-O-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3.5 h / Heating / reflux

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: Heating / reflux

3.1: hydrazine / ethanol / 2 h / Heating / reflux

4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 0 - 20 °C

5.1: caesium carbonate / N,N-dimethyl-formamide / 2.5 h / 20 °C

6.1: hydrogen / palladium on carbon / ethanol / 2.5 h / 20 °C / 2585.81 Torr

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydrogen; sodium hydride; caesium carbonate; triphenylphosphine; hydrazine; diethylazodicarboxylate; palladium on carbon; In tetrahydrofuran; tetrachloromethane; ethanol; N,N-dimethyl-formamide; toluene;