potassium (2,3-dimethylphenyl)trifluoroborate

Base Information

• Chemical Name: potassium (2,3-dimethylphenyl)trifluoroborate
• CAS No.: 1412414-17-5
• Molecular Formula: C₈H₉BF₃*K
• Molecular Weight: 212.064

Synonyms:potassium (2,3-dimethylphenyl)trifluoroborate

Chemical Property of potassium (2,3-dimethylphenyl)trifluoroborate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Potassium 2,3-dimethylphenyltrifluoroborate >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of potassium (2,3-dimethylphenyl)trifluoroborate

There total 2 articles about potassium (2,3-dimethylphenyl)trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

potassium hydrogen difluoride + 2,3-dimethylphenylboronic acid (183158-34-1) → potassium (2,3-dimethylphenyl)trifluoroborate (1412414-17-5)

Guidance literature:

In water; acetonitrile; for 0.25h;

DOI:10.1021/acs.orglett.6b01159

Reference yield: 99.0%

2,3-dimethylphenylboronic acid (183158-34-1) → potassium (2,3-dimethylphenyl)trifluoroborate (1412414-17-5)

Guidance literature:

With potassium hydrogen difluoride; In diethyl ether; water; at 20 ℃; for 3h;

DOI:10.1002/anie.201503528

Reference yield: 80.0%

potassium (2,3-dimethylphenyl)trifluoroborate (1412414-17-5) + (E)-4-(benzo[d][1,3]dioxol-5-yl)but-3-en-2-one (22214-31-9) → 4-(benzo[d][1,3]dioxo-5-yl)-4-(2,3-dimethylphenyl)butan-2-one

Guidance literature:

With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; lithium bromide; In toluene; at 111 ℃; for 48h; enantioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.201503528

upstream raw materials:

2,3-dimethylphenylboronic acid

Downstream raw materials:

1,2-dimethyl-3-(trifluoromethyl)benzene

3-fluoro-o-xylene

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