C₂₃H₃₄N₂O₈

Base Information

Chemical Name:C₂₃H₃₄N₂O₈
CAS No.:1407508-30-8
Molecular Formula:C₂₃H₃₄N₂O₈
Molecular Weight:466.532
Hs Code.:

C<sub>23</sub>H<sub>34</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₂₃H₃₄N₂O₈

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Chemical Property of C₂₃H₃₄N₂O₈

Chemical Property:

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Technology Process of C₂₃H₃₄N₂O₈

There total 8 articles about C₂₃H₃₄N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1407508-26-2
C₂₉H₄₈N₂O₈Si

: 1407508-30-8
C₂₃H₃₄N₂O₈

Guidance literature:: C₂₉H₄₈N₂O₈Si; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With water; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2012.08.008

Reference yield:

: 626201-36-3
(2R,3R,5R,6R)-5,6-dimethoxy-5,6-dimethyl-1,4-dioxane-2,3-dicarbothioic acid di-S-ethyl ester

: 1407508-30-8
C₂₃H₃₄N₂O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.25 h / -78 °C

1.3: 0 - 20 °C

2.1: titanium(IV) isopropylate / 240 h / 100 °C / Inert atmosphere; Sealed tube

3.1: lithium aluminium tetrahydride / 70 °C

4.1: sodium hydride / tetrahydrofuran; pentane / 20 °C

4.2: 20 °C

5.1: di-isopropyl azodicarboxylate; triphenylphosphine; hydrogen azide / tetrahydrofuran; benzene / 0 - 20 °C / Inert atmosphere

6.1: hydrogen; 10% Pd/C / ethyl acetate; ethanol / 3 h / 2585.81 Torr

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; lithium aluminium tetrahydride; hydrogen azide; di-isopropyl azodicarboxylate; 10% Pd/C; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; pentane; benzene; 5.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetasy.2012.08.008

Reference yield:

: 243964-13-8
[(2R,3S,5R,6R)-3-(hydroxymethyl)-5,6-dimethoxy-5,6-dimethyl-1,4-dioxan-2-yl]methanol

: 1407508-30-8
C₂₃H₃₄N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; pentane / 20 °C

1.2: 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine; hydrogen azide / tetrahydrofuran; benzene / 0 - 20 °C / Inert atmosphere

3.1: hydrogen; 10% Pd/C / ethyl acetate; ethanol / 3 h / 2585.81 Torr

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With hydrogen azide; di-isopropyl azodicarboxylate; 10% Pd/C; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; pentane; benzene; 2.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetasy.2012.08.008