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3-chloro-3-(2-formylphenyl)diazirine hydrazone

Base Information
  • Chemical Name:3-chloro-3-(2-formylphenyl)diazirine hydrazone
  • CAS No.:864667-73-2
  • Molecular Formula:C8H7ClN4
  • Molecular Weight:194.623
  • Hs Code.:
3-chloro-3-(2-formylphenyl)diazirine hydrazone

Synonyms:3-chloro-3-(2-formylphenyl)diazirine hydrazone

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Chemical Property of 3-chloro-3-(2-formylphenyl)diazirine hydrazone
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Technology Process of 3-chloro-3-(2-formylphenyl)diazirine hydrazone

There total 2 articles about 3-chloro-3-(2-formylphenyl)diazirine hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrazine hydrate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo0512204
Guidance literature:
Multi-step reaction with 2 steps
1: 63 percent / diisopropylaluminium hydride / hexane / 1 h / -77 °C
2: 92 percent / hydrazine hydrate / CH2Cl2 / 3 h / 20 °C
With diisopropyl aluminum hydride; hydrazine hydrate; In hexane; dichloromethane;
DOI:10.1021/jo0512204
Guidance literature:
With manganese(IV) oxide; In dichloromethane; for 0.166667h; cooling;
DOI:10.1021/jo0512204
upstream raw materials:

3-chloro-3-(2-formylphenyl)diazirine

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