C₅₉H₆₃N₁₃O₁₂S₆

Base Information

Chemical Name:C₅₉H₆₃N₁₃O₁₂S₆
CAS No.:1361395-25-6
Molecular Formula:C₅₉H₆₃N₁₃O₁₂S₆
Molecular Weight:1338.63
Hs Code.:

C<sub>59</sub>H<sub>63</sub>N<sub>13</sub>O<sub>12</sub>S<sub>6</sub>

Synonyms:C₅₉H₆₃N₁₃O₁₂S₆

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Chemical Property of C₅₉H₆₃N₁₃O₁₂S₆

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Technology Process of C₅₉H₆₃N₁₃O₁₂S₆

There total 6 articles about C₅₉H₆₃N₁₃O₁₂S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1361395-24-5
C₅₇H₆₁N₁₃O₁₁S₆

: 108-24-7
acetic anhydride

: 1361395-25-6
C₅₉H₆₃N₁₃O₁₂S₆

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃;
DOI:10.1021/jm201685h

Reference yield:

: 960061-69-2
C₄₈H₄₃N₁₅O₈S₆

: 1361395-25-6
C₅₉H₆₃N₁₃O₁₂S₆

Guidance literature:: Multi-step reaction with 3 steps

1: 12 h / 80 °C

2: pyridine; dmap / dichloromethane / 3 h

3: caesium carbonate / N,N-dimethyl-formamide / 2 h

With pyridine; dmap; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide; 1: Curtius rearrangement;
DOI:10.1021/jm201685h

Reference yield:

: C₅₆H₅₄N₁₄O₁₁S₆

: 1361395-25-6
C₅₉H₆₃N₁₃O₁₂S₆

Guidance literature:: Multi-step reaction with 6 steps

1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C

2: triethylamine / acetone / 1 h / Sonication

3: sodium azide / acetone / 1.33 h / 60 °C

4: 12 h / 80 °C

5: pyridine; dmap / dichloromethane / 3 h

6: caesium carbonate / N,N-dimethyl-formamide / 2 h

With pyridine; dmap; sodium azide; water; caesium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 4: Curtius rearrangement;
DOI:10.1021/jm201685h