C₃₄H₄₅FN₂O₅Si₂

Base Information

Chemical Name:C₃₄H₄₅FN₂O₅Si₂
CAS No.:1445380-08-4
Molecular Formula:C₃₄H₄₅FN₂O₅Si₂
Molecular Weight:636.911
Hs Code.:

C<sub>34</sub>H<sub>45</sub>FN<sub>2</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₄H₄₅FN₂O₅Si₂

Suppliers and Price of C₃₄H₄₅FN₂O₅Si₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₃₄H₄₅FN₂O₅Si₂

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of C₃₄H₄₅FN₂O₅Si₂

There total 10 articles about C₃₄H₄₅FN₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445380-06-2
C₃₄H₄₅FN₂O₆Si₂

: 1445380-08-4
C₃₄H₄₅FN₂O₅Si₂

Guidance literature:: C₃₄H₄₅FN₂O₆Si₂; With pyridine; methyl chloroformate; In dichloromethane; at 20 ℃; for 1h;

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tributylphosphine; ammonium formate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 1445379-59-8
2’-deoxy-2’-fluoro-3’-O-(tert-butyldimethylsilyl)uridine

: 1445380-08-4
C₃₄H₄₅FN₂O₅Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 3 h / Reflux

2.1: sodium hydroxide / 1,4-dioxane; water / 2 h / 20 °C

2.2: 0.5 h / 20 °C / pH 7

3.1: pyridine / dichloromethane / 14 h / 0 - 20 °C

4.1: 1H-imidazole / dichloromethane / 14 h / 20 °C

4.2: 15 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

6.1: tetrahydrofuran / 3 h / -78 - 0 °C

7.1: pyridine; methyl chloroformate / dichloromethane / 1 h / 20 °C

7.2: 0.5 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; Dess-Martin periodane; methyl chloroformate; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile;

Reference yield:

: 1445379-61-2
4'-α-methylhydroxyl-3'-tert-butyldimethylsilyl-2'-deoxy-2'-fluorouridine

: 1445380-08-4
C₃₄H₄₅FN₂O₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 14 h / 0 - 20 °C

2.1: 1H-imidazole / dichloromethane / 14 h / 20 °C

2.2: 15 h / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 3 h / -78 - 0 °C

5.1: pyridine; methyl chloroformate / dichloromethane / 1 h / 20 °C

5.2: 0.5 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; Dess-Martin periodane; methyl chloroformate; In tetrahydrofuran; dichloromethane;