6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine

Base Information

Chemical Name:6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine
CAS No.:178484-21-4
Molecular Formula:C₃₈H₅₀N₄O₁₂
Molecular Weight:754.835
Hs Code.:

Synonyms:6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine

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Chemical Property of 6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine

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Technology Process of 6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine

There total 2 articles about 6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 6-<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3-chloropyridazine

: 178484-21-4
6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine

Guidance literature:: With Ni(TPP)4; In N,N-dimethyl-formamide; at 50 ℃; for 12h;
DOI:10.1055/s-1996-4255

Reference yield:

: 96574-04-8
2-(2-(2-(2-(4-methoxyphenoxy)ethoxy)ethoxy)ethoxy)ethan-1-ol

: 178484-21-4
6,6'-bis<11-((4-methoxyphenyl)oxy)-3,6,9-trioxaundecyl-1-oxy>-3,3'-bipyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / NaH / toluene / 3 h / 80 °C

2: 47 percent / Ni(TPP)4 / dimethylformamide / 12 h / 50 °C

With Ni(TPP)4; sodium hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-1996-4255