3-(2,3,4-Trimethoxyphenyl)propanal

Base Information

Chemical Name:3-(2,3,4-Trimethoxyphenyl)propanal
CAS No.:261619-90-3
Molecular Formula:C12H16 O4
Molecular Weight:224.257
Hs Code.:
DSSTox Substance ID:DTXSID10448095
Nikkaji Number:J2.514.668I
Mol file:261619-90-3.mol

Synonyms:3-(2,3,4-trimethoxyphenyl)propanal;261619-90-3;3-(2,3,4-TRIMETHOXY-PHENYL)-PROPIONALDEHYDE;2,3,4-Trimethoxybenzenepropanal;DTXSID10448095;EN300-1841710

Suppliers and Price of 3-(2,3,4-Trimethoxyphenyl)propanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-(2,3,4-TRIMETHOXY-PHENYL)-PROPIONALDEHYDE 95.00%
5MG
$ 496.80

Total 2 raw suppliers

Chemical Property of 3-(2,3,4-Trimethoxyphenyl)propanal

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Refractive Index:1.495
Boiling Point:306.42°C at 760 mmHg
Flash Point:131.626°C
Density:1.078g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:224.10485899
Heavy Atom Count:16
Complexity:207

Purity/Quality:

97% ^*data from raw suppliers

3-(2,3,4-TRIMETHOXY-PHENYL)-PROPIONALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)CCC=O)OC)OC

Technology Process of 3-(2,3,4-Trimethoxyphenyl)propanal

There total 2 articles about 3-(2,3,4-Trimethoxyphenyl)propanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 152821-16-4
2,2-dimethyl-5-<(2,3,4-trimethoxyphenyl)-methylene>-1,3-dioxane-4,6-dione

: 261619-90-3
3-(2,3,4-trimethoxyphenyl)propanal

Guidance literature:: 2,2-dimethyl-5-<(2,3,4-trimethoxyphenyl)-methylene>-1,3-dioxane-4,6-dione; With phenylsilane; 4-methylmorpholine N-oxide; hexacarbonyl molybdenum; In tetrahydrofuran; at 80 ℃; for 16h;

With water; In tetrahydrofuran; at 20 ℃; for 0.25h; Further stages.;
DOI:10.1021/ol701812w

Reference yield:

: 2103-57-3
2,3,4-trimethoxybenzaldehyde

: 261619-90-3
3-(2,3,4-trimethoxyphenyl)propanal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 69 percent / H₂O / 2 h / 75 °C

2.1: N-methylmorpholine-N-oxide; PhSiH₃ / Mo(CO)6 / tetrahydrofuran / 16 h / 80 °C

2.2: 48 percent / H₂O / tetrahydrofuran / 0.25 h / 20 °C

With phenylsilane; 4-methylmorpholine N-oxide; hexacarbonyl molybdenum; In tetrahydrofuran; water; 1.1: Knoevenagel condensation;
DOI:10.1021/ol701812w