N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

Base Information

Chemical Name:N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid
CAS No.:110512-51-1
Molecular Formula:C₂₀H₂₉N₃O₈
Molecular Weight:439.466
Hs Code.:

Synonyms:N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

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Chemical Property of N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

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Technology Process of N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

There total 7 articles about N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,4R,5R,6R)-6-{(R)-2-[(S)-2-((S)-2-Benzyloxycarbonylamino-propionylamino)-3-phenyl-propionylamino]-1-hydroxy-ethyl}-4,5-dihydroxy-tetrahydro-pyran-2-carboxylic acid

: 110512-51-1
N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; under 2250.2 - 3000.2 Torr; Yield given;
DOI:10.1021/jm00395a022

Reference yield:

: 20911-65-3
N-Cbz-L-alanyl-L-phenylalanine succinimido ester

: 110512-51-1
N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / triethylamine / methanol; tetrahydrofuran / 3 h / Ambient temperature

2: LiOH / H₂O; tetrahydrofuran; dimethylformamide

3: H₂ / 10percent Pd/C / H₂O; tetrahydrofuran / 2250.2 - 3000.2 Torr

With lithium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00395a022

Reference yield:

: 2768-53-8
N-benzyloxycarbonyl-L-alanyl-L-phenylalanine

: 110512-51-1
N-(L-alanyl-L-phenylalanyl)-8-amino-2,6-anhydro-3,8-dideoxy-D-glycero-D-talo-octonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: dicyclocarbodiimide / tetrahydrofuran / 0 - 5 °C

2: 31 percent / triethylamine / methanol; tetrahydrofuran / 3 h / Ambient temperature

3: LiOH / H₂O; tetrahydrofuran; dimethylformamide

4: H₂ / 10percent Pd/C / H₂O; tetrahydrofuran / 2250.2 - 3000.2 Torr

With lithium hydroxide; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00395a022