2,4,6-triisopropylphenyl tripropynyltin

Base Information

Chemical Name:2,4,6-triisopropylphenyl tripropynyltin
CAS No.:883970-29-4
Molecular Formula:C₂₄H₃₂Sn
Molecular Weight:439.228
Hs Code.:

Synonyms:2,4,6-triisopropylphenyl tripropynyltin

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Chemical Property of 2,4,6-triisopropylphenyl tripropynyltin

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Technology Process of 2,4,6-triisopropylphenyl tripropynyltin

There total 1 articles about 2,4,6-triisopropylphenyl tripropynyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1083008-01-8
(C₆H₂(CH(CH₃)2)3)SnCl₃

: 74-99-7
prop-1-yne

: 883970-29-4
2,4,6-triisopropylphenyl tripropynyltin

Guidance literature:: With n-BuLi; In toluene; (N2); propyne condensed in toluene at -196°C; soln. of BuLi in toluene added dropwise at -90°C; slowly warmed to room temp.; stirred for 15 min; cooled to -90°C; soln. of Sn compd. in toluene added dropwise; warmed; stirred for 12 h; filtered through MgSO4; volatiles removed (vac.); elem. anal.;
DOI:10.1016/j.jorganchem.2008.07.036

Reference yield: 43.0%

: 883970-29-4
2,4,6-triisopropylphenyl tripropynyltin

: 6192-52-5
p-toluenesulfonic acid monohydrate

: 7732-18-5
water

: 108-88-3,15644-74-3,16713-13-6
toluene

: ([2,4,6-iPr3C6H2Sn-(μ2-OH)-(eta.2μ2)-p-MeC6H4SO3]3(μ3-O))(4-MeC6H4SO3)*2toluene

Guidance literature:: In tetrahydrofuran; to soln. Sn-compound in THF water was added at room temp., mixt. was heated under reflux for 9 days, 4-MeC6H4SO3H*H2O was added at room temp., mixt. was refluxed for 6 h; mixt. was dried under reduced pressure, solid was dissolved in toluene, filtered; elem. anal.;
DOI:10.1039/b706377f

Reference yield: 32.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 883970-29-4
2,4,6-triisopropylphenyl tripropynyltin

: 6192-52-5
p-toluenesulfonic acid monohydrate

: 7732-18-5
water

: [(C₆H₂(CH(CH₃)2)3)Sn(OH)(O₃SC₆H₄CH₃)2]2(H₂O)*1.5C₄H₈O

Guidance literature:: In tetrahydrofuran; water; (N2); H2O (12 equiv.) was added to stirred soln. of Sn compd. in THF; refluxed for 8 d; acid was added at room temp.; refluxed for 6 h; dried (vac.); dissolved in THF; filtered; cooled to 10°C; elem. anal.;
DOI:10.1016/j.jorganchem.2008.07.036