C₁₄H₇Br₃N₆

Base Information

Chemical Name:C₁₄H₇Br₃N₆
CAS No.:1346428-26-9
Molecular Formula:C₁₄H₇Br₃N₆
Molecular Weight:498.962
Hs Code.:

C<sub>14</sub>H<sub>7</sub>Br<sub>3</sub>N<sub>6</sub>

Synonyms:C₁₄H₇Br₃N₆

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Chemical Property of C₁₄H₇Br₃N₆

Chemical Property:

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Technology Process of C₁₄H₇Br₃N₆

There total 4 articles about C₁₄H₇Br₃N₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63516-03-0
α-bromo-p-toluidine

: 1346428-26-9
C₁₄H₇Br₃N₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine; copper(ll) bromide / acetonitrile / 1 h / 50 °C

1.2: 0.5 h

2.1: sodium azide / N,N-dimethyl-formamide

3.1: copper(ll) sulfate pentahydrate; sodium ascorbate / tetrahydrofuran; water / 16 h / 60 °C

With sodium azide; copper(ll) sulfate pentahydrate; bromine; sodium ascorbate; copper(ll) bromide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; 3.1: Sharpless cycloaddition;
DOI:10.1016/j.bmcl.2011.08.073

Reference yield:

: 1213234-82-2
3,4,5-tribromobenzyl azide

: 1346428-05-4
C₇H₃N₃

: 1346428-26-9
C₁₄H₇Br₃N₆

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium ascorbate; In tetrahydrofuran; water; at 60 ℃; for 16h;
DOI:10.1016/j.bmcl.2011.08.073

Reference yield:

: 81278-48-0
1-(bromomethyl)-3,4,5-tribromobenzene

: 1346428-26-9
C₁₄H₇Br₃N₆

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide

2: copper(ll) sulfate pentahydrate; sodium ascorbate / tetrahydrofuran; water / 16 h / 60 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium ascorbate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 2: Sharpless cycloaddition;
DOI:10.1016/j.bmcl.2011.08.073