Technology Process of C14H7Br3N6
There total 4 articles about C14H7Br3N6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bromine; copper(ll) bromide / acetonitrile / 1 h / 50 °C
1.2: 0.5 h
2.1: sodium azide / N,N-dimethyl-formamide
3.1: copper(ll) sulfate pentahydrate; sodium ascorbate / tetrahydrofuran; water / 16 h / 60 °C
With
sodium azide; copper(ll) sulfate pentahydrate; bromine; sodium ascorbate; copper(ll) bromide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
3.1: Sharpless cycloaddition;
DOI:10.1016/j.bmcl.2011.08.073
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium ascorbate;
In
tetrahydrofuran; water;
at 60 ℃;
for 16h;
DOI:10.1016/j.bmcl.2011.08.073
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / N,N-dimethyl-formamide
2: copper(ll) sulfate pentahydrate; sodium ascorbate / tetrahydrofuran; water / 16 h / 60 °C
With
sodium azide; copper(ll) sulfate pentahydrate; sodium ascorbate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
2: Sharpless cycloaddition;
DOI:10.1016/j.bmcl.2011.08.073