mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)}

Base Information

• Chemical Name: mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)}
• CAS No.: 56085-32-6
• Molecular Formula: C₅₃H₄₄MoO₃P₄
• Molecular Weight: 948.766

Synonyms:mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)}

Chemical Property of mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)}

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Technology Process of mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)}

There total 1 articles about mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

fac-bis{bis(diphenylphosphino)methane}tricarbonylmolydenum (56009-06-4) → mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)} (56085-32-6)

Guidance literature:

With tetrafluoroboric acid diethyl ether; triethylamine; In dichloromethane; slight excess of HBF4*Et2O; treatment with NEt3;;

DOI:10.1039/c39870001778

Reference yield: 89.0%

mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)} (56085-32-6) + ((CN)Ag(P(C6H5)3)) → (OC)3Mo((C6H5)4P2CH2)2AgCN

Guidance literature:

In dichloromethane; Ag(PPh3)CN was added to a stirred soln. of complex in CH2Cl2, mixt. was stirred for 5 min;; light petroleum was added, soln. was reduced in volume, ppt. was sepd.; elem. anal.;;

Reference yield: 87.0%

trans-chlorohydridobis(triphenylphosphine)platinum(II) (16841-99-9,25879-12-3,16902-93-5) + mer-{Mo(CO)3(η2-bis(diphenylphosphino)methane)(η1-bis(diphenylphosphino)methane)} (56085-32-6) → {(CO)3Mo(μ-bis(diphenylphosphino)methane)2PtH(Cl)}*0.5(benzene)

Guidance literature:

With benzene; In benzene; trans-PtH(Cl)(PPh3)2 added to soln. of Mo complex in hot C6H6 under N2, refluxed for 5 min, allowed to cool; evapd. under vac., triturated with Et2O; elem. anal.;

DOI:10.1039/DT9870000221

upstream raw materials:

fac-bis{bis(diphenylphosphino)methane}tricarbonylmolydenum

Downstream raw materials:

(Mo(CO)2(NCS)2(Ph₂PCH₂PPh₂-PP')(Ph₂PCH₂PPh₂-P))

{MoPdCl(μ-Cl)(CO)2(μ-CO)(μ-bis(diphenylphosphino)methane)2}

gold

((CH₃)3CNC)(CO)3Mo((C₆H₅)2PCH₂P(C₆H₅)2)2PdCl⁽¹⁺⁾*Cl^(1-)={((CH₃)3CNC)(CO)3Mo((C₆H₅)2PCH₂P(C₆H₅)2)2PdCl}Cl

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