N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

Base Information

Chemical Name:N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide
CAS No.:213684-78-7
Molecular Formula:C₂₅H₃₂N₂O₃S
Molecular Weight:440.607
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

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Chemical Property of N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

Chemical Property:

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Technology Process of N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

There total 7 articles about N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 6-((4-(benzyloxy)benzo[d]oxazol-2-yl)thio)-N-(2,6-diisopropylphenyl)hexanamide

: 213684-78-7
N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

Guidance literature:: With thiophenol; trifluoroacetic acid; at 20 ℃; for 12h; Cooling with ice;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 213685-59-7
2-nitroresorcinol monobenzyl ether

: 213684-78-7
N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; zinc / 1 h / 20 °C

2: ethanol / 24 h / Reflux

3: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 1.5 h / 80 °C

4: thiophenol; trifluoroacetic acid / 12 h / 20 °C / Cooling with ice

With 18-crown-6 ether; potassium carbonate; acetic acid; thiophenol; trifluoroacetic acid; zinc; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 213685-50-8
2-amino-3-(benzyloxy)phenol

: 213684-78-7
N-(2,6-diisopropylphenyl)-6-((4-hydroxybenzo[d]oxazol-2-yl)thio)hexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 24 h / Reflux

2: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 1.5 h / 80 °C

3: thiophenol; trifluoroacetic acid / 12 h / 20 °C / Cooling with ice

With 18-crown-6 ether; potassium carbonate; thiophenol; trifluoroacetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.06.024