(2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride

Base Information

• Chemical Name: (2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride
• CAS No.: 1623432-63-2
• Molecular Formula: C₅H₁₁NO*ClH
• Molecular Weight: 137.609
• Hs Code.: 2921490090

Synonyms:(2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride

Chemical Property of (2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

(2S)-2-amino-2-cyclopropylethan-1-olhcl 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of (2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride

There total 2 articles about (2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H19NO2S → (2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride (1623432-63-2)

Guidance literature:

With hydrogenchloride; In methanol; at 20 ℃; for 2h;

DOI:10.1021/acs.jmedchem.7b00621

Reference yield:

C14H31NO2SSi → (2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride (1623432-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydrogencarbonate; dihydrogen peroxide; potassium fluoride / methanol; tetrahydrofuran / 2 h / 0 - 45 °C / Inert atmosphere

2: hydrogenchloride / methanol / 2 h / 20 °C

With hydrogenchloride; potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol;

DOI:10.1021/acs.jmedchem.7b00621

Reference yield: 100.0%

(2S)-2-amino-2-cyclopropylethan-1-ol hydrochloride (1623432-63-2) → (S)-2-amino-2-cyclopropylethan-1-ol (1198185-81-7)

Guidance literature:

With sodium methylate; In methanol; at 0 ℃; Inert atmosphere;

DOI:10.1021/jm501550p

Downstream raw materials:

methyl 4-(2-((3R,5R,6S)-1-((S)-2-(tert-butylsulfonyl)-1-cyclopropylethyl)-6-(4-chloro-3-fluorophenyl)-5-(3-chlorophenyl)-3-methyl-2-oxopiperidin-3-yl)acetamido)-2-methoxybenzoate

4-(2-((3R,5R,6S)-1-((S)-2-(tert-butylsulfonyl)-1-cyclopropylethyl)-6-(4-chloro-3-fluorophenyl)-5-(3-chlorophenyl)-3-methyl-2-oxopiperidin-3-yl)acetamido)-2-methoxybenzoic acid

(S)-2-amino-2-cyclopropylethan-1-ol

(3S,5R,6S)-3-allyl-6-(4-chloro-3-fluorophenyl)-5-(3-chlorophenyl)-1-((S)-1-cyclopropyl-2-hydroxyethyl)-3-methylpiperidin-2-one

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