methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside
CAS No.:1248566-33-7
Molecular Formula:C₂₉H₄₁NO₇Si
Molecular Weight:543.733
Hs Code.:

Synonyms:methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

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Chemical Property of methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

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Technology Process of methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

There total 1 articles about methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1248566-32-6
methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsily-4-C-cyano-2,4-dideoxy-α-D-glucopyranoside

: 1248566-33-7
methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

Guidance literature:: methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsily-4-C-cyano-2,4-dideoxy-α-D-glucopyranoside; With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 2.66667h;

With water; potassium bitartrate; In dichloromethane; toluene; at 20 ℃; for 0.25h;
DOI:10.1016/j.carres.2010.05.032

Reference yield: 82.0%

: 1248566-33-7
methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

: 1248566-73-5
benzyl (3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate

: 1248566-76-8
C₆₉H₈₅N₅O₁₄Si

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 18h;
DOI:10.1016/j.carres.2010.05.032

Reference yield: 81.0%

: 1248566-10-0
methyl (3S,4R)-4-acetoxypyrrolidine-3-carboxylate

: 1248566-33-7
methyl 3-O-benzyl-2-N-(benzyloxycarbonyl)amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-4-C-formyl-α-D-glucopyranoside

: 1248566-37-1
methyl 4-C-[(3S,4R)-4-acetoxy-3-(methoxycarbonyl)-pyrrolidin-1-yl]methyl-3-O-benzyl-2-(benzyloxycarbonyl)-amino-6-O-tert-butyldimethylsilyl-2,4-dideoxy-α-D-glucopyranoside

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.carres.2010.05.032