4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

Base Information

Chemical Name:4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide
CAS No.:1416804-00-6
Molecular Formula:C₂₅H₃₂N₂O₄S
Molecular Weight:456.606
Hs Code.:

Synonyms:4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

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Chemical Property of 4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

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Technology Process of 4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

There total 4 articles about 4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1416803-96-7
2-(4-chlorobutoxy)benzo[d]thiazole

: 146978-52-1
4-hydroxy-3-methoxy-N,N-bis(1-methylethyl)benzenecarboxamide

: 1416804-00-6
4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

Guidance literature:: 4-hydroxy-3-methoxy-N,N-bis(1-methylethyl)benzenecarboxamide; With sodium hydroxide; In N,N-dimethyl-formamide; at 50 - 55 ℃; for 0.5h;

2-(4-chlorobutoxy)benzo[d]thiazole; In N,N-dimethyl-formamide; at 80 - 90 ℃; for 3h;
DOI:10.1007/s12272-015-0672-x

Reference yield:

: 121-34-6
3-methoxy-4-hydroxybenzoic acid

: 1416804-00-6
4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 1 h / Reflux

1.2: 2 h / 20 °C / Cooling with ice

2.1: sodium hydroxide / N,N-dimethyl-formamide / 0.5 h / 50 - 55 °C

2.2: 3 h / 80 - 90 °C

With thionyl chloride; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s12272-015-0672-x

Reference yield:

: 934-34-9
2-hydroxybenzothiazole

: 1416804-00-6
4-(4-(benzo[d]thiazol-2-yloxy)butoxy)-N,N-diisopropyl-3-methoxy benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 0.5 h / 50 - 55 °C

1.2: 3 h / 80 - 90 °C

2.1: sodium hydroxide / N,N-dimethyl-formamide / 0.5 h / 50 - 55 °C

2.2: 3 h / 80 - 90 °C

With potassium carbonate; sodium hydroxide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s12272-015-0672-x