9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

Base Information

Chemical Name:9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin
CAS No.:1236182-58-3
Molecular Formula:C₂₀H₁₆N₆
Molecular Weight:340.387
Hs Code.:

Synonyms:9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

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Chemical Property of 9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

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Technology Process of 9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

There total 5 articles about 9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 73568-27-1
2-chloro-6-methylquinoline-3-carbaldehyde

: 36072-62-5
3-benzyl-4,5-diamino-1,2,3-triazole

: 1236182-58-3
9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

Guidance literature:: for 0.0833333h; Microwave irradiation; Ionic liquid;
DOI:10.1016/j.bmcl.2011.06.007

Reference yield:

: 29313-28-8
1-phenylacetyl-thiosemicarbazide

: 1236182-58-3
9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid

2: hydrazine hydrate / ethanol / Reflux

3: 0.08 h / Microwave irradiation; Ionic liquid

With sulfuric acid; hydrazine hydrate; In ethanol;
DOI:10.1016/j.bmcl.2011.06.007

Reference yield:

: 937-39-3
2-phenylacetylhydrazine

: 1236182-58-3
9-(4-methyl)-5-benzyl-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepin

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / water / Heating

2: sulfuric acid

3: hydrazine hydrate / ethanol / Reflux

4: 0.08 h / Microwave irradiation; Ionic liquid

With hydrogenchloride; sulfuric acid; hydrazine hydrate; In ethanol; water;
DOI:10.1016/j.bmcl.2011.06.007