Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ⁵-phospha-indan-1-ylidene)-amine

Base Information

• Chemical Name: Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ⁵-phospha-indan-1-ylidene)-amine
• CAS No.: 178879-56-6
• Molecular Formula: C₂₁H₁₄F₆NOP
• Molecular Weight: 441.312

Synonyms:Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ⁵-phospha-indan-1-ylidene)-amine

Chemical Property of Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ⁵-phospha-indan-1-ylidene)-amine

Chemical Property:

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Technology Process of Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ⁵-phospha-indan-1-ylidene)-amine

There total 7 articles about Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ⁵-phospha-indan-1-ylidene)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C35H26F6NOP (178879-54-4,178963-22-9) → 1,1-Diphenylethylene (530-48-3) + Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ5-phospha-indan-1-ylidene)-amine (178879-56-6)

Guidance literature:

In ⁽²⁾H₈-toluene; at 200 ℃; for 120h; Yield given;

Reference yield:

N-(diphenylmethylidene)phenylamine (574-45-8) → Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ5-phospha-indan-1-ylidene)-amine (178879-56-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) n-BuLi / 2.) THF, 0 deg C

2: 73 percent / Ph₃P, EtO₂CN=NCO₂Et

3: toluene-d8 / 120 h / 200 °C

With n-butyllithium; triphenylphosphine; diethylazodicarboxylate; In ⁽²⁾H₈-toluene;

DOI:10.1080/10426509608545197

Reference yield:

2-(methylphenylphosphinyl)-α,α-bis(trifluoromethyl)phenylmethanol (140658-12-4) → Phenyl-(1-phenyl-3,3-bis-trifluoromethyl-2-oxa-1λ5-phospha-indan-1-ylidene)-amine (178879-56-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) n-BuLi / 2.) THF, 0 deg C

2: 73 percent / Ph₃P, EtO₂CN=NCO₂Et

3: toluene-d8 / 120 h / 200 °C

With n-butyllithium; triphenylphosphine; diethylazodicarboxylate; In ⁽²⁾H₈-toluene;

DOI:10.1080/10426509608545197

upstream raw materials:

C₃₅H₂₆F₆NOP

C₃₇H₂₈F₆NO₃P

N-(diphenylmethylidene)phenylamine

2-(methylphenylphosphinyl)-α,α-bis(trifluoromethyl)phenylmethanol

Downstream raw materials:

1-Phenyl-3,3-bis-trifluoromethyl-2-oxa-1-phospha-indan 1-oxide

aniline

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